Study of nanomechanical properties of (1-y)BST-yMgO thin films

ISSN: 0870-8312

Ciência & Tecnologia dos Materiais is the official journal of SPM, the Portuguese Society of Materials (Sociedade Portuguesa de Materiais), providing a forum for publishing peer-reviewed papers related to both fundamentals of materials science and technological application of engineering materials. The scope of the journal covers a wide range of topics in materials science that are of interest to the SPM, encompassing electrochemistry, corrosion and protection of materials, extractive metallurgy and recycling, electronic and optoelectronic materials, biomaterials, forest materials, polymeric and composite materials, foundry, heat treatment and surface engineering, tribology, and fracture. Science and Technology of Materials welcomes contributions in the form of original research papers, review articles and technical notes reporting advances on those fields, emphasizing new materials, new products and devices, and new technologies.

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In the present study thin films of MgO – modified Ba0.6Sr0.4TiO3 (BST60/40) solid solution were prepared by the sol-gel-type chemical solution deposition method on stainless steel substrates. A multilayer spin-coating approach was utilized for the Ba0.6Sr0.4TiO3-MgO thin film deposition with subsequent thermal annealing at T=650-750°C. Dried BST60/40-MgO gel powders were studied with thermogravimetric and differential thermal analysis to determine their thermochemical properties. X-ray diffraction analysis was utilized for thin film characterization in terms of its phase composition and crystal structure. The influence of y=1, 3 and 5 mol.% MgO doping on nanomechanical properties of BST60/40 thin films was studied with nanoindentation. It was found that BST6040 thin films adopted the tetragonal P4mm (99) structure. The volume of the BST60/40 elementary cell, the average hardness as well as the mean value of the Young modulus decreased with an increase in amount of MgO.

Keywords:

BST thin films

sol-gel method

crystal structure

AFM

nanoindentation

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